A practical core cleaning method based on CO2 dissolved gas drive
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摘要: 为了提高岩心的洗油效率,开发了一种实用的CO2溶解气驱岩心洗油方法。该方法在Stewart设计的CO2溶解气驱方法的基础上,增加了洗油室抽真空、CO2预清洗、溶剂回收3个步骤。使用自行研制的DGO-1型CO2溶解气驱洗油装置,实验考察了新方法的洗油效果。6块不同孔隙度、渗透率的岩心的洗油结果表明,经过6~10次CO2溶解气驱后,岩心荧光级别均小于3级,孔隙度和渗透率趋于稳定,可满足石油天然气行业标准SY/T 5336-2006的要求,且洗油时间(2~3天)较常规脂肪抽提洗油(2~3周或更长)有大幅度减少。该方法洗油原理清楚,洗油装置简单,易于操作,洗油效率高,清洁环保,推荐作为一种实用方法在岩石物理实验室推广使用。Abstract: In order to improve the efficiency of core cleaning, a practical core cleaning method based on CO2 dissolved gas drive was developed. The method added vacuum-pumping, CO2 pre-cleaning and solvent recovery to the method designed by Stewart in 1952. Then, the effect of core cleaning was observed through a series of experiment with the employment of DGO-1 type CO2 dissolved gas drive core cleaning device which was self-made. The results of core cleaning of 6 rocks with different porosities and permeabilities showed that the fluorescence level was less than 3 and the porosity and permeability were steady after 6-10 circles. The effect met the standard SY/T 5336-2006. The period of core cleaning with the employment of the new method was 2-3 days, which was less than that of Soxhlet extraction device (2-3 weeks or longer). Since the method had the characteristics of clear principle, simple device, good operability, high efficiency and was environmental-friendly, it was recommended to popularize in rock physics lab.
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Key words:
- CO2 dissolved gas drive /
- core cleaning /
- CO2 pre-cleaning /
- fluorescence level /
- porosity /
- permeability
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