多芳烃参数定量评价烃源岩成熟度的方法——以银额盆地中生界烃源岩为例

陈治军; 张亚雄; 王永昌; 王希; 葛宏选; 高志亮; 李子梁

doi:10.11781/sysydz202201139

多芳烃参数定量评价烃源岩成熟度的方法——以银额盆地中生界烃源岩为例

doi: 10.11781/sysydz202201139

陈治军^{1, 2,},
张亚雄^3, ,,
王永昌⁴,
王希⁴,
葛宏选²,
高志亮²,
李子梁²

1.
长江大学资源与环境学院, 武汉 430100
2.
陕西延长石油(集团)有限责任公司研究院, 西安 710075
3.
中国石化石油勘探开发研究院, 北京 100083
4.
中国石油集团渤海钻探工程有限公司定向井分公司, 天津 300280

基金项目:

国土资源部重点项目“十三五全国油气资源评价” 2017YQZYPJ01

延长集团科技攻关项目“银额盆地哈日凹陷主力烃源岩生烃特征与资源潜力分析” ycsy2020jcyjB-03

详细信息

作者简介:
陈治军(1980-), 男, 博士研究生, 高级工程师, 从事油气地球化学研究。E-mail: chenzhijun2203@aliyun.com

通讯作者:
张亚雄(1983-), 男, 博士, 高级工程师, 从事石油地质学、沉积学研究工作。E-mail: 157498674@qq.com

中图分类号: TE122.1
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出版历程
- 收稿日期: 2021-08-09
- 修回日期: 2021-12-03
- 刊出日期: 2022-01-28

Quantitative assessment of source rock maturity with multiple aromatic parameters: a case study of Mesozoic source rocks in Yingen-Ejinaqi Basin

1.
College of Resources and Environment, Yangtze University, Wuhan, Hubei 430100, China
2.
Reseach Institute of Yanchang Petroleum (Group) Co. Ltd., Xi'an, Shaanxi 710075, China
3.
SINOPEC Petroleum Exploration and Production Research Institute, Beijing 100083, China
4.
Directional Drilling Company, Bohai Drilling Company, CNPC, Tianjin 300280, China

摘要

摘要: 芳烃成熟度参数被广泛应用于评价烃源岩或原油成熟度，但实际上生源特征、沉积环境等因素对一些参数的影响可能大于成熟度的控制，导致一些参数在某些研究区的应用效果并不理想，且前人基于单一参数建立的计算视镜质体反射率（R_c）的关系式也并不适用于所有研究区，因此，探索出了一种芳烃参数定量评价烃源岩成熟度的方法。该方法基于研究区一定数量的烃源岩芳烃组分的色谱—质谱（GC-MS）分析数据，通过开展各芳烃成熟度参数与R_o的相关性分析，分别在烷基萘系列、烷基菲系列和烷基二苯并噻吩系列3大类芳烃成熟度参数中找出1个对成熟度最敏感（相关系数最大）的参数，利用数值分析软件对这几个参数和R_o进行多元线性回归，拟合出一个利用多参数定量计算R_c的关系式。该方法在银额盆地哈日凹陷中生界湖相混合型（有机质类型以Ⅱ₁—Ⅱ₂型为主）烃源岩研究中取得了很好的应用效果。用该方法拟合出的关系式计算的R_c与R_o的相关系数R²高达0.96，相对于单一芳烃参数，相关系数有了大幅度的提高，表明该方法具有可靠性。
- 芳烃成熟度参数 /
- 多元回归法 /
- 定量评价 /
- 烃源岩成熟度 /
- 银额盆地
Abstract: Aromatic parameters have been widely applied to assess the maturity of organic matters. Some parameters may not only be affected by maturation, but also more affected by organic matter source, sedimentary environment, etc. Therefore, the application effect of some parameters in some study areas were not satisfying, and the previous relational expression to calculate the vitrinite reflectance (R_c) which only based on a single parameter is also not suitable for other areas. In this study, we proposed a method to improve the accuracy of using multiple aromatic parameters to quantitatively evaluate source rock maturity. This method was based on a certain number of GC-MS analysis data of aromatic fractions of source rocks in the study area, to find out a most sensitive parameter to maturity in three categories of aromatics (alkyl naphthalene series, alkyl phenanthrene series and alkyl dibenzothiophene series) respectively. Here the most sensitive parameter meant having the largest correlation coefficient to R_o in certain category. Then a multiple linear regression equation was established among these three parameters and R_o using a numerical analysis software, and with this equation R_c can then be calculated with multiple parameters. This method is applied to the study of Mesozoic lacustrine source rocks in the Hari Sag of Yingen-Ejinaqi Basin, the organic matter types of these source rock are mainly type Ⅱ₁-Ⅱ₂. The results indicated that the correlation coefficient (R_c) between R_o and R_c which was calculated by established formula was as high as 0.96, and compared with the single aromatics parameter, the correlation coefficient has been considerably improved.
- maturity parameters of polycyclic aromatic /
- multiple regression method /
- quantitative evaluation /
- maturity of source rock /
- Yingen-Ejinaqi Basin

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图 1 萘、菲和二苯并噻吩碳骨架型式

据文献[15, 18]修改。

Figure 1. Carbon skeleton pattern of naphthalene, phenanthrene and dibenzothiophene compounds

下载: 全尺寸图片幻灯片

图 2 银额旗盆地哈日凹陷构造位置及相关取样井

Figure 2. Tectonic location of Hari Sag in Yingen-Ejinaqi Basin and relevant sampling wells

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图 3 银额盆地哈日凹陷中生界湖相烃源岩样品的TOC(a)、S₁+S₂(b)分布频率直方图

Figure 3. Distribution frequency of TOC (a) and S₁+S₂ (b) of lacustrine source rock samples from Mesozoic, Hari Sag, Yingen-Ejinaqi Basin

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图 4 银额盆地哈日凹陷中生界湖相烃源岩样品有机质类型划分

底图据文献[32-33]。

Figure 4. Organic matter types of lacustrine source rock samples from Mesozoic, Hari Sag, Yingen-Ejinaqi Basin

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图 5 银额盆地哈日凹陷中生界湖相烃源岩样品芳烃系列相对含量

Figure 5. Component of polycyclic aromatic compounds of lacustrine source rock samples from Mesozoic, Hari Sag, Yingen-Ejinaqi Basin

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图 6 银额盆地哈日凹陷中生界湖相烃源岩芳烃参数与R_o相关关系

Figure 6. Correlation between maturity parameters of polycyclic aromatic and R_o of lacustrine source rock samples from Mesozoic, Hari Sag, Yingen-Ejinaqi Basin

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图 7 银额盆地哈日凹陷中生界湖相烃源岩样品新模型计算的R_c与R_o相关关系

Figure 7. Correlation between R_c calculated by the new model and R_o of lacustrine source rock samples from Mesozoic, Hari Sag, Yingen-Ejinaqi Basin

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表 1 芳烃成熟度参数

Table 1. Maturity parameters of aromatic hydrocarbons

参数类别	参数代号	表达式	资料来源
烷基萘类	MNR	2-MN/1-MN	文献[1]
	DNR-1	(2，6-DMN+2，7-DMN)/1，5-DMN	文献[1]
	DNR-2	2，7-DMN/1，8-DMN	文献[1]
	DNR-3	2，6-DMN/1，8-DMN	文献[1]
	DNR-4	1，7-DMN/1，8-DMN	文献[1]
	DNR-5	1，6-DMN/1，8-DMN	文献[1]
	TMNr	2，3，6-TMN/(1，4，6-TMN+1，2，5-TMN)	文献[1]
	TMNr1	2，3，6-TMN/(1，4，6-TMN+1，3，5-TMN)	文献[1]
	TMNr2	(2，3，6-TMN+1，3，7-TMN)/(1，4，6-TMN+1，3，5-TMN+1，3，6-TMN)	文献[1]
	TMNr3	1，3，7-TMN/(1，3，7-TMN+1，2，5-TMN)	文献[1]
	TeMNr	1，3，6，7-TeMN/(1，3，6，7-TeMN+1，2，5，7-TeMN)	文献[1]
	PMNr	1，2，4，6，7-PMN/(1，2，4，6，7-PMN +1，2，3，5，6-PMN)	文献[1]
烷基菲类	MPI1	1.5×(2-MP+3-MP)/(P+1-MP+9-MP)	文献[7]
	MPI2	3×(2-MP)/(P+1-MP+9-MP)	文献[7]
	MPI3	(2-MP+ 3-MP)/(1-MP+9-MP)	文献[5]
	MPR	(2-MP)/ (1-MP)	文献[1]
	F₁	(3-MP + 2-MP) /(1-MP + 2-MP + 3-MP + 9-MP)	文献[9]
	F₂	2-MP /(1-MP + 2-MP + 3-MP + 9-MP)	文献[9]
	DPR	(2，6-MP+2，7-MP)/(1，6-MP+2, 10-MP)	文献[2]
	DPR2	2，7-MP/1，8-MP	文献[5]
烷基二苯并噻吩类	MDR	4-MDBT/1-MDBT	文献[12-13]
	MDBI	4-MDBT/(DBT+1-MDBT+2-MDBT+3-MDBT+4-MDBT)	文献[14]
	DMDBT1	4，6-DMDBT/1，4-DMDBT	文献[10, 12]
	DMDBT2	2，4-DMDBT/1，4-DMDBT	文献[10, 12]
	DMDBT3	2，6-DMDBT/1，4-DMDBT	文献[10, 12]
	DMDBT4	4，6- DMDBT /(1，4- DMDBT +1，6- DMDBT)	文献[11]
	DMDBT5	(2，6 - DMDBT+3，6- DMDBT)/(1，4- DMDBT + 1，6 - DMDBT)	文献[11]
注：MN.甲基萘；DMN.二甲基萘；TMN.三甲基萘；TeMN.四甲基萘；PMN.五甲基萘；P.菲；MP.甲基菲；DBT.二苯并噻吩；MDBT.甲基二苯并噻吩；DMDBT.二甲基二苯并噻吩

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