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陆相页岩层系岩心含水量现场分析技术及初步应用

贾梦瑶 鲍云杰 李志明 冷筠滢 刘旺威 何晋译 卢龙飞 黎茂稳

贾梦瑶, 鲍云杰, 李志明, 冷筠滢, 刘旺威, 何晋译, 卢龙飞, 黎茂稳. 陆相页岩层系岩心含水量现场分析技术及初步应用[J]. 石油实验地质, 2024, 46(2): 420-427. doi: 10.11781/sysydz202402420
引用本文: 贾梦瑶, 鲍云杰, 李志明, 冷筠滢, 刘旺威, 何晋译, 卢龙飞, 黎茂稳. 陆相页岩层系岩心含水量现场分析技术及初步应用[J]. 石油实验地质, 2024, 46(2): 420-427. doi: 10.11781/sysydz202402420
JIA Mengyao, BAO Yunjie, LI Zhiming, LENG Junying, LIU Wangwei, HE Jinyi, LU Longfei, LI Maowen. Technique and preliminary application of field analysis of water content for continental shale cores[J]. PETROLEUM GEOLOGY & EXPERIMENT, 2024, 46(2): 420-427. doi: 10.11781/sysydz202402420
Citation: JIA Mengyao, BAO Yunjie, LI Zhiming, LENG Junying, LIU Wangwei, HE Jinyi, LU Longfei, LI Maowen. Technique and preliminary application of field analysis of water content for continental shale cores[J]. PETROLEUM GEOLOGY & EXPERIMENT, 2024, 46(2): 420-427. doi: 10.11781/sysydz202402420

陆相页岩层系岩心含水量现场分析技术及初步应用

doi: 10.11781/sysydz202402420
基金项目: 

中国石化“十四五”资源评价方法与数据库建设项目 P23229

国家自然科学基金项目 42090022

详细信息
    作者简介:

    贾梦瑶(1994—),女,工程师,从事页岩油气评价研究。E-mail:jiamy975.syky@sinopec.com

    通讯作者:

    鲍云杰(1963—),男,研究员,从事测试技术与页岩油气评价研究。E-mail:baoyj.syky@sinopec.com

  • 中图分类号: TE135

Technique and preliminary application of field analysis of water content for continental shale cores

  • 摘要: 陆相页岩层系的流体分析是页岩油选层评价的重要基础。针对陆相页岩层系流体表征技术的现状和钻井现场的需求,基于岩心样品中水分易于散失的特性,探索建立了适用于井场基于微波的岩样含水快速测试方法。岩心出筒擦除表面的钻井液之后,第一时间采集具有代表性的块状岩样加载到破碎主机上破碎处理呈颗粒状,将颗粒状的样品倒入加载到微波含水测定仪的样品杯中,2 s后即可得到岩样水分的质量分数,测试绝对误差平均0.15%。初步应用研究表明:一是岩样水分检测结果可以转换为水分在样品孔隙系统中占据的孔隙空间,结合井场热解等资料快速计算样品的视孔隙度,为井场决策提供数据支撑;二是结合岩样块密度和热解数据等资料,计算岩心样品的视含油饱和度和视含水饱和度,实现井场岩样流体的快速评价。该方法的应用不需要对岩样进行洗油和烘干处理,缩短了分析周期,丰富了适用于井场的岩心孔隙度、流体分析实验技术手段和方法。

     

  • 图  1  我国不同盆地陆相页岩层系页岩油甜点含油饱和度分布特征

    据参考文献[9, 19, 24]修改。

    Figure  1.  Distribution characteristics of oil saturation in shale oil sweet spots of continental shale layers in various basin in China

    图  2  材料的含水率与微波相移和衰减的关系

    据参考文献[35]修改。

    Figure  2.  Relationship between moisture content and microwave phase shift and attenuation of the material

    图  3  微波含水分析仪组成示意

    Figure  3.  Schematic diagram of microwave water analyzer

    图  4  利用含水量和游离油含量(S1)计算视孔隙度图版

    Figure  4.  Apparent porosity chart calculated using water content and free oil content (S1)

    图  5  利用含水量和游离油含量(S1) 计算视含油饱和度图版

    Figure  5.  Apparent oil saturation chart calculated using water content and free oil content (S1)

    表  1  柱塞样品与颗粒状样品含水测定数据对比

    Table  1.   Comparison of water content determination data between plunger and granular samples

    样品号 柱塞样含水率/% 颗粒样含水率/% 绝对误差/ % 平均绝对误差/%
    1 1.52 1.67 -0.15 0.24
    2 1.92 1.93 -0.01
    3 1.63 1.61 0.03
    4 0.24 0.45 -0.22
    5 2.84 2.36 0.48
    6 3.85 4.00 -0.15
    7 2.36 2.73 -0.37
    8 3.10 3.41 -0.30
    9 5.70 5.73 -0.03
    10 4.43 3.82 0.62
    下载: 导出CSV

    表  2  标准样品含水量标称值与实测值数据对比

    Table  2.   Comparison of nominal and measured water content data of standard sample

    项目 样品号
    1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
    标称值/% 0.80 0.76 1.25 1.07 1.10 1.99 1.38 1.88 1.75 2.28 1.62 3.05 2.28 2.74 2.26
    实测值/% 0.79 0.76 1.25 1.19 1.11 2.02 1.20 1.95 1.41 2.01 1.95 2.90 2.41 2.24 2.31
    绝对误差/% 0.00 0.00 0.00 0.12 0.01 0.03 0.18 0.07 0.34 0.27 0.33 0.14 0.12 0.50 0.05
    下载: 导出CSV
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  • 收稿日期:  2023-04-24
  • 修回日期:  2024-02-20
  • 刊出日期:  2024-03-28

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